Synthesis of chitosan-based resins modified with tris(2-aminoethyl)amine moiety and its application to collection/concentration and determination of trace mercury by inductively coupled plasma atomic emission spectrometry

Lukman Hakim; Akhmad Sabarudin; Koji Oshita; Mitsuko Oshima; Shoji Motomizu

doi:10.1016/j.talanta.2008.05.025

Synthesis of chitosan-based resins modified with tris(2-aminoethyl)amine moiety and its application to collection/concentration and determination of trace mercury by inductively coupled plasma atomic emission spectrometry

Lukman Hakim
, Akhmad Sabarudin
, Koji Oshita
, Mitsuko Oshima
, Shoji Motomizu^*

^*Corresponding author for this work

Research output: Contribution to journal › Article › peer-review

42 Citations (Scopus)

Abstract

A novel chitosan-based chelating resin modified with tris(2-aminoethyl)amine moiety (CCTS-TAA) was synthesized, and its characteristics in the collection/concentration of mercury was examined. The synthesized resin showed good adsorption toward mercury in a wide pH range, and the adsorbed mercury can be easily eluted by using 2 M HNO₃ without any addition of complexing agent. The resin was then packed in a mini-column and the mini-column was installed on a computer-controlled automated-pretreatment (Auto-Pret) system coupled with inductively coupled plasma-atomic emission spectroscopy (ICP-AES) for on-line mercury collection and determination at trace level.

Original language	English
Pages (from-to)	1256-1260
Number of pages	5
Journal	Talanta
Volume	76
Issue number	5
DOIs	https://doi.org/10.1016/j.talanta.2008.05.025
Publication status	Published - 15 Sept 2008
Externally published	Yes

Keywords

Chitosan
Computer control
Inductively coupled plasma-atomic emission spectrometry
Mercury
On-line pretreatment
Resin
Tris(2-aminoethyl)amine moiety

Access to Document

10.1016/j.talanta.2008.05.025

Fingerprint

Dive into the research topics of 'Synthesis of chitosan-based resins modified with tris(2-aminoethyl)amine moiety and its application to collection/concentration and determination of trace mercury by inductively coupled plasma atomic emission spectrometry'. Together they form a unique fingerprint.

Cite this

@article{483bf70e3cf34afc9a19033fdf7550d0,

title = "Synthesis of chitosan-based resins modified with tris(2-aminoethyl)amine moiety and its application to collection/concentration and determination of trace mercury by inductively coupled plasma atomic emission spectrometry",

abstract = "A novel chitosan-based chelating resin modified with tris(2-aminoethyl)amine moiety (CCTS-TAA) was synthesized, and its characteristics in the collection/concentration of mercury was examined. The synthesized resin showed good adsorption toward mercury in a wide pH range, and the adsorbed mercury can be easily eluted by using 2 M HNO3 without any addition of complexing agent. The resin was then packed in a mini-column and the mini-column was installed on a computer-controlled automated-pretreatment (Auto-Pret) system coupled with inductively coupled plasma-atomic emission spectroscopy (ICP-AES) for on-line mercury collection and determination at trace level.",

keywords = "Chitosan, Computer control, Inductively coupled plasma-atomic emission spectrometry, Mercury, On-line pretreatment, Resin, Tris(2-aminoethyl)amine moiety",

author = "Lukman Hakim and Akhmad Sabarudin and Koji Oshita and Mitsuko Oshima and Shoji Motomizu",

year = "2008",

month = sep,

day = "15",

doi = "10.1016/j.talanta.2008.05.025",

language = "English",

volume = "76",

pages = "1256--1260",

journal = "Talanta",

issn = "0039-9140",

publisher = "Elsevier B.V.",

number = "5",

}

Hakim, L , Sabarudin, A, Oshita, K, Oshima, M & Motomizu, S 2008, 'Synthesis of chitosan-based resins modified with tris(2-aminoethyl)amine moiety and its application to collection/concentration and determination of trace mercury by inductively coupled plasma atomic emission spectrometry', Talanta, vol. 76, no. 5, pp. 1256-1260. https://doi.org/10.1016/j.talanta.2008.05.025

Synthesis of chitosan-based resins modified with tris(2-aminoethyl)amine moiety and its application to collection/concentration and determination of trace mercury by inductively coupled plasma atomic emission spectrometry. / Hakim, Lukman ; Sabarudin, Akhmad; Oshita, Koji et al.
In: Talanta, Vol. 76, No. 5, 15.09.2008, p. 1256-1260.

Research output: Contribution to journal › Article › peer-review

TY - JOUR

T1 - Synthesis of chitosan-based resins modified with tris(2-aminoethyl)amine moiety and its application to collection/concentration and determination of trace mercury by inductively coupled plasma atomic emission spectrometry

AU - Hakim, Lukman

AU - Sabarudin, Akhmad

AU - Oshita, Koji

AU - Oshima, Mitsuko

AU - Motomizu, Shoji

PY - 2008/9/15

Y1 - 2008/9/15

N2 - A novel chitosan-based chelating resin modified with tris(2-aminoethyl)amine moiety (CCTS-TAA) was synthesized, and its characteristics in the collection/concentration of mercury was examined. The synthesized resin showed good adsorption toward mercury in a wide pH range, and the adsorbed mercury can be easily eluted by using 2 M HNO3 without any addition of complexing agent. The resin was then packed in a mini-column and the mini-column was installed on a computer-controlled automated-pretreatment (Auto-Pret) system coupled with inductively coupled plasma-atomic emission spectroscopy (ICP-AES) for on-line mercury collection and determination at trace level.

AB - A novel chitosan-based chelating resin modified with tris(2-aminoethyl)amine moiety (CCTS-TAA) was synthesized, and its characteristics in the collection/concentration of mercury was examined. The synthesized resin showed good adsorption toward mercury in a wide pH range, and the adsorbed mercury can be easily eluted by using 2 M HNO3 without any addition of complexing agent. The resin was then packed in a mini-column and the mini-column was installed on a computer-controlled automated-pretreatment (Auto-Pret) system coupled with inductively coupled plasma-atomic emission spectroscopy (ICP-AES) for on-line mercury collection and determination at trace level.

KW - Chitosan

KW - Computer control

KW - Inductively coupled plasma-atomic emission spectrometry

KW - Mercury

KW - On-line pretreatment

KW - Resin

KW - Tris(2-aminoethyl)amine moiety

UR - https://www.scopus.com/pages/publications/50149104738

U2 - 10.1016/j.talanta.2008.05.025

DO - 10.1016/j.talanta.2008.05.025

M3 - Article

C2 - 18761187

AN - SCOPUS:50149104738

SN - 0039-9140

VL - 76

SP - 1256

EP - 1260

JO - Talanta

JF - Talanta

IS - 5

ER -

Synthesis of chitosan-based resins modified with tris(2-aminoethyl)amine moiety and its application to collection/concentration and determination of trace mercury by inductively coupled plasma atomic emission spectrometry

Abstract

Keywords

Access to Document

Other files and links

Fingerprint

Cite this